o:3371 Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS en A new GC‑MS/MS method from the ISO 18363 series of standards for determination of fatty acid bound hloropropanediols and glycidol was assessed for its performance characteristics. This method enables indirect simultaneous determination of free 2‑monochloropro‑ pane‑1,3‑diol (2‑MCPD), 3‑monochloropropane‑1,2‑diol (3‑MCPD) and glycidol in a single sample preparation and analysis protocol. Results of the validation study show satisfactory performance characteristics, well within required limits. Recently held proficiency testing also showed the adequate performance of the laboratories employing this method. Taking into consideration the simpler sample preparation and stringent quality control inherent to this protocol, wider use of ISO 18363:4:2021 for routine applications can be expected in the foreseeable future. MCPD, Glycidol, Ester, Oil ,GC‑MS/MS 1552099 10.18485/meattech.2023.64.2.91 2023-11-28T08:58:58.632Z 44 yes 46 Srdjan Stefanović Institute of meat Hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS Saša Janković Institute of Meat Hygiene and Technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person Nikola Borjan Institute of meat hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person Stefan Simunović Institute of meat hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person Radivoj Petronijević Instiute of meat hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person Dejana Trbović Institute of meat hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person Čaba Siladji Instiute of meat hygiene and technology Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS person 2023-11-03 application/pdf 397073 https://unilib.phaidrabg.rs/o:3371 no yes 16 70 92000001 71A01 Meat technology 64 Special Issue 64 2 475 479 Kaćanskog 13, 11 000 Belgrade Institute of Meat Hygiene and Technology 2023-11-03