MCPD, Glycidol, Ester, Oil ,GC‑MS/MS eng 2023-11-03 Institute of Meat Hygiene and Technology info:eu-repo/semantics/article A new GC‑MS/MS method from the ISO 18363 series of standards for determination of fatty acid bound hloropropanediols and glycidol was assessed for its performance characteristics. This method enables indirect simultaneous determination of free 2‑monochloropro‑ pane‑1,3‑diol (2‑MCPD), 3‑monochloropropane‑1,2‑diol (3‑MCPD) and glycidol in a single sample preparation and analysis protocol. Results of the validation study show satisfactory performance characteristics, well within required limits. Recently held proficiency testing also showed the adequate performance of the laboratories employing this method. Taking into consideration the simpler sample preparation and stringent quality control inherent to this protocol, wider use of ISO 18363:4:2021 for routine applications can be expected in the foreseeable future. http://creativecommons.org/licenses/by/4.0/legalcode Stefanović, Srdjan Janković, Saša Borjan, Nikola Simunović, Stefan Petronijević, Radivoj Trbović, Dejana Siladji, Čaba Performance evaluation of the ISO 18363-4:2021 method for quantitative determination of chloropropanediols and glycidol in fats and oils by GC-MS/MS Meat technology 64(2) https://unilib.phaidrabg.rs/o:3371 doi:10.18485/meattech.2023.64.2.91 application/pdf 397073 bytes